Amino Acids, Peptides and Proteins (SPR Amino Acids, by J. S. Davies

By J. S. Davies

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By J. S. Davies

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Aronova, N. N. Makhova, and S. I. Zavialov, Izvest. Akad. , Ser. , 1970, 1835. R. Knorr and R. Huisgen, Chem. , 1970, 103, 2598. K. Unaheim and M. Gacek, Acta Chem. , 1969, 2488, 2475. T. Invi, S. Tanaka, and M. Takino, Bull. Chem. Japan, 1970, 43, 1582. l~~ Previous attempts to prepare these compounds via the acid chloride had been unsuccessful. - (yAGH \ RZ--C >C-CO,H R1 I 0 2 II ‘N-0 &NO h V > / NO, NO2 ,R? ‘C NO2 (54) (53) ring-opening and decarboxylation to (54). l’~ C. ~~~ Hydrogenolysis of aryl-2-oxazolines of the type (56) affords N-formylphenylalanine ethyl esters in good yield.

1970,70, 561. G. A. Olah, D. L. Brydon, and R. H. Schlosberg, J. Org. , 1970, 35, 317. Lijinsky, L. Keefer, and J. Loo, Tetrahedron, 1970, 26, 5137. K. Heyns and H. Koch, Tetrahedron Letters, 1970, 741. H. 0. Bayer, H. Gotthardt, and R. Huisgen, Chem. , 1970, 103,2356. R. Huisgen, H. Gotthardt, and H. 0. Bayer, Chem. , 1970, 103,2368. 0. Bayer, R. Huisgen, R. Knorr, and F. C. Schaefer, Chem. , 1970,103,2581. R. Huisgen, H. Gotthardt, H. 0. Bayer, and F. C. Schaefer, Chem. , 1970, 103, 2611. l~~9 166 Reaction of (46) with acetic anhydride containing appreciable amounts of acetic acid yields (47) which then COzH I PhCy COPh N' Me 0Ph N Me Ph COMe affords the normal Dakin-West product (48).

Kalmanson, Biochem. Biophys. Acta, 1970, 200, 160. T. Jellinek and R. B. Johns, Photochem. , 1970, 11, 349. G. Gennari and G. S. Letters, 1970, 10, 129. G. Jori and G. Cauzzo, Photochem. , 1970, 12, 231. 208 5 Analytical Methods The number of papers on the subject of amino-acids which are devoted to analytical methods continues to run at approximately a quarter of the total published. g. amino-acids in biological fluids), The improvements and developments in amino-acid analysis in relation to structural studies of proteins and peptides are also covered elsewhere in this Report (Chap.

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